Critus

Bulk Reflection Geometry

Suitable for most laboratory based x-ray diffractometers and synchrotron sources. For example*: Bruker D8, Rigaku SmartLab, Pan-Analytical Empyrean and X'Pert.

Description

The Reflection Geometry system allows electric fields of ±5kV to be applied to bulk materials while conducting XRD measurements from a surface. Ideal for electro-ceramic and single crystal research in laboratory or synchrotron x-ray systems. Electrical current and displacements sensors are packaged within the unit allowing simultaneous strain and polarization measurements.

Specifications

  • Suitable for most laboratory based x-ray diffractometers and synchrotron sources
    • For example: Bruker D8, Rigaku SmartLab, Pan-Analytical Empyrean and X'Pert
  • Mechanical strain and electrical polarisation measurements in situ
  • Applied voltages ±5 kV
    • Recommended external amplifier is the Trek 10/10B-HS, although custom cabling for alternative amplifiers is possible upon request
    • Silicon oil can be used in horizontal geometry to increase achievable field
  • Sample diameters of 7 mm to 12 mm
  • Sample thicknesses of 0.1 mm to 2 mm
  • Temperature range from room temperature to 200°C
  • Large scattering angle range, including grazing incidence angles
  • Compact system design for maximum portability and versatility
  • Interlocked for safety with voltage application only possible when cell is closed

Please Note

Compatibility of a particular diffractometer will depend on its configuration. Please discuss with our contact staff to understand if your system is suitable.